ÚTEF - Ústav technické a experimentální fyziky ČVUT - České vysoké učení technické v Praze
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ÚTEF - Ústav technické a experimentální fyziky ČVUT - České vysoké učení technické v Praze
ČVUT - České vysoké učení technické v Praze
Publikace  > Články v impaktovaných časopisech  > 'Non-destructive imaging of framents of historical beeswax seals using high-contrast X-ray micro-radiography and micro-tomography with large area photon-counting detector array'
Non-destructive imaging of framents of historical beeswax seals using high-contrast X-ray micro-radiography and micro-tomography with large area photon-counting detector array

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Rok
2016

Časopis
Micron (accepted)

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Obsah
Historic beeswax seals are unique cultural heritage objects. Unfortunately, a number of historical sealing waxes show a porous structure, with a strong tendency to stratification and embrittlement, which makes these objects extremely prone to mechanical damage. The understanding of beeswax degradation processes therefore plays an important role in the preservation and consequent treatment of these objects. Conventional methods applied for the investigation of beeswax materials (e.g. gas chromatography) are of a destructive nature or bring only limited information about the sample surface (microscopic techniques). Considering practical limitations of conventional methods and ethical difficulties connected with the sampling of the historical material, radiation imaging methods such as X-ray micro-tomography presents a promising non-destructive tool for the onward scientific research in this field. In this contribution, we present the application of high-contrast X-ray micro-radiography and micro-tomography for the investigation of beeswax seal fragments. The method is based on the application of the large area photon-counting detector recently developed at our institute. The detector combines the advantages of single-photon counting technology with a large field of view. The method, consequently, enables imaging of relatively large objects with high geometrical magnification. In the reconstructed micro-tomographies of investigated historical beeswax seals, we are able to reveal morphological structures such as stratification, micro-cavities and micro-fractures with spatial resolution down to 10 µm non-destructively and with high imaging quality. The presented work therefore demonstrates that a combination of state-of-the-art hybrid pixel semiconductor detectors and currently available micro-focus x-ray sources makes it possible to apply X-ray micro-radiography and micro-tomography as a valuable non-destructive tool for volumetric beeswax seal morphological studies.
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Příklad citace článku:
J. Karch, B. Bartl, J. Dudák, J. Žemlička, F. Krejčí, "Non-destructive imaging of framents of historical beeswax seals using high-contrast X-ray micro-radiography and micro-tomography with large area photon-counting detector array", Micron (accepted) (2016)

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